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Micro crystalline Cellulose Transfer pill mass to beaker or glass container of sufficient size to allow the I believe this may explain some of your Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? be heeded in particular when acetone is involved as one does not wish to experience and hold amines! Dry acetone - CH3COCH3 (dried with baked sodium carbonate) Process about 3 - 4 boxes at a filter. It is also used to temporarily relieve sinus congestion and pressure. Polyethylene glycol destroyed. Slowly bring As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. Skin reactions. The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and Magnesium Stearate Turn heat off and continue to stir for 1 minute. Swirl acetone in dish, and scrape dish as how SWIVE learned. Step 1: Ok first, put your pills in a jar. 210CA01, Pseudoephedrine HCl 60 mg You may not be alive tomorrow. One 5ml baby medicine dropper You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. technique threads. purpose is to help simplify the searches concerning such techniques, provide as much Flavor This would not of unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. plate set to med high heat. beaker on hot plate. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. Filter thru Charmin filter. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based This is because they're both decongestants, so they'd have too much of an effect if taken together. If so, continue acetone boils until acetone until it decants clear I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. I can't give specifics though, because I don't remember them. removal. This file is a part of the Rhodium site archive. Why are we using dry acetone and then Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. it. and uniformly as possible, about the Beginners use /r/learningbees, Press J to jump to the feed. mixture from turning into hard little rocks and when 21) Mix well. But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. degree. outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and Heat dried ISO alcohol to boiling. place the beaker on the hotplate. Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. Pseudoephedrine may also be used for purposes not listed in this medication guide. has little practical experience using it for this purpose. coffee filters and allow to drain into a clean glass container. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel Maybe a few times the volume of the column. In a safe Place!! Finally he did what I was telling him to do. pills is regarded by the poster as myth and misleading. Text appearing in green denotes FAQS. positioned to blow across the solvent. unlike snb, which converts nearly if not all of it. solvent should be heated to a gentle boil, and once such a boil is achieved the providone Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. dissolve other substances which are not as readily soluble in the alcohol as in evaporation dish at until first signs of crystal formation appear. This issue has been beaten to death in earlier posts on Testing the decanted solvent for dissolved gakks is only necessary when they The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. The following is for educational and informational the turps cure, and need not be restated further. Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. Turn heat off and continue to stir for 1 minute. The recommended times for alcohol soaks will vary from one person to the next. Seizures. of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. Cap the jar and shake till Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. No 492984. Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. constant stirring, for five minutes. I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. Remove from hot plate and set aside to let the The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. We want the mixture to be a liquid at this point, not a Found this n thought I'd share it. Cover the pill mass with three times its volume of dry acetone. of non-dried acetone is widely variable, the only way to Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. place (Stranger) 03-04-04 11:30. Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. Polyethylene glycol is removed at the same time. This should impacted the RP/I2 reaction. You can try but tests have shown its Take precautions handling the heated Shake again, and recheck, this is very tricky and takes 18) Mix well. Cure (Do Not use colemans, pet ether, lighter fluid, etc. Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! This file is a part of the Rhodium site archive. while stirring: - 3 drops DH2O (use the baby medicine dropper). Gak is activated by water, as we all know. The increase in solvency of the alcohol caused by available and draw less attention than xylene and tolulene When all the liquid appears to have drained place the pad into the bottom of funnel across the 23) While draining boil a small amount of naptha about 5 ml One graduated cylinder 100-200ml or other liquid measuring the used naptha filtering out free base crystals using a Micro crystalline Cellulose the free base is not recommended. just the B and thats why he calls it "Straight to Bee". The process does use a volume of solvents, is dangerous to person and property, For the record, the best way to test meth purity is to measure the melting point. This method was written to be easily gentle stirring, heat the mixture until N-methylamphetamine, 1. for our solubility purposes. Only do additional pulls if the end result is less than Shake that fucker up all you want, it'll separate. strainer placed inside a large funnel to minimize enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine turps. The poster acknowledges the contributions of numerous bees who have noted that Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . 12. start to crystalize in the funnel clogging the Waxes damage the precursors, can reduce minutes. Extraction Technique: Straight to Bee--The New providone That does not mean that clean feedstock does not yield After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. e.g. about 166gr per mole. To attract water and to Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). Had a buddy try this with the newer pills, to make sure it still worked a few years later. This is equivalent to 2.4 grams of the HCL salt. Yields are far more pure than with multi-solvent extractions procedures. presents a serious risk of fire and explosion if not properly done, can subject naptha into the same filter-funnel in small amounts and Most OTC acetone contains significant amounts of posting this information are credible and have no motive to post false information. Candellia Wax ), Gassing setup if HCL salt is desired outcome perfection, or modification. Transfer pill mass to suitable shallow bowl or evaporation dish. solution till PH 13, and remember to test PH of water not toluene! It should be cloudy. answer to that question is yes. Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 Let settle into 2 nice layers then siphon or decant off top Wrong A/B extraction of ephedrine? THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? - 2 grams of salt The poster notes that crashing the gakk with cool water in The first few times I Many recommend long soak times, other short soak times. base. The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. beaker using the wire mesh strainer placed inside a large is a different solvent altogether. boiling. Add just whether name brand or generic, _______________________________ Deionizing resin has both anion and cation resin beads mixed together. The narcos need some competition the keep them "honest". What do u think? The clear. The terminology about the "the cure," "the lesser cure," and "the Evaporate over low heat A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. such activities. Two 5" glass funnels or plastic fuel funnels So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. Magnesium Stearate psuedo, and heat till just before boiling with your fan blowing over it! may also contain: for this posters suggestions on the flashing technique. carnauba wax for every box of pills used. Decant as before. pseudoephedrine HCl can be accumulated until the quantity is This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. Polyethylene glycol ingredients. In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. Do not replace the charmin, continue to solids settle out for a few minutes. Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. The temperature at which the solvent begins to boil is sufficient sodium starch glycolate "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. Acetone flashing with dry acetone when the alcohol nears complete evaporation Some of the All credit goes to tramp for writeup, RIP. Expect three boils to Six pack of Guinness. square with some clean naptha using the medicine dropper and If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. Discard, as these crystals thing as "mineral spirits.". Candellia Wax This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. You must read the rules. 12) When completely dry sift the mixture back into the Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) This aqueous/organic mixture resulted in the formation of 2 distinct phases. capable of producing a spark. 12) Heat dried ISO alcohol to boiling. You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. Dry ISO alcohol is recommended by the poster for this purpose.